Part 3 · Chapter 25

Hydrocarbons

The carbon-and-hydrogen backbone of organic chemistry — unreactive alkanes, electron-rich alkenes and alkynes, and the special stability of the benzene ring

Fundamentals of Chemistry Prof. Mithun Mondal Reading time ≈ 65 min
i What you'll learn
  • How hydrocarbons divide into alkanes, alkenes, alkynes and aromatics.
  • Key preparations — Wurtz, decarboxylation, dehydrohalogenation, dehydration.
  • The free-radical halogenation mechanism and electrophilic addition to alkenes.
  • Markovnikov's rule and the anti-Markovnikov peroxide effect.
  • The acidity of terminal alkynes and the chemistry of ozonolysis.
  • Aromaticity (Hückel's rule), electrophilic aromatic substitution, and directing effects.
Section 25-1

Classifying Hydrocarbons

Hydrocarbons contain only carbon and hydrogen. They split into saturated (alkanes, all single bonds), unsaturated (alkenes with \(\ce{C=C}\), alkynes with \(\ce{C#C}\)) and aromatic (benzene and its relatives). The degree of unsaturation governs reactivity: alkanes resist most reagents, while the electron-rich multiple bonds invite attack.

ClassBondingGeneral formulaTypical reaction
AlkaneC–C single\(\ce{C_nH_{2n+2}}\)free-radical substitution
Alkeneone \(\ce{C=C}\)\(\ce{C_nH_{2n}}\)electrophilic addition
Alkyneone \(\ce{C#C}\)\(\ce{C_nH_{2n-2}}\)addition; terminal acidity
Aromaticdelocalised ring(e.g. \(\ce{C6H6}\))electrophilic substitution
Section 25-2

Alkanes: Preparation

Alkanes — the "paraffins" (Latin parum affinis, little affinity) — are made by lengthening or shortening carbon chains, or by reducing unsaturation.

MethodReaction
Wurtz reaction\(\ce{2R-X + 2Na -> R-R + 2NaX}\)
Hydrogenation\(\ce{CH2=CH2 + H2 ->[Ni] CH3CH3}\)
Decarboxylation\(\ce{CH3COONa + NaOH ->[\Delta] CH4 + Na2CO3}\)
Reduction of \(\ce{R-X}\)\(\ce{R-X + 2[H] ->[Zn/HCl] R-H + HX}\)
Wurtz limitation. Because two identical radicals combine best, the Wurtz reaction is reliable only for symmetrical alkanes. Using two different halides gives a messy mixture of all three possible coupling products.
Section 25-3

Alkanes: Free-Radical Halogenation

The signature alkane reaction is substitution by halogens in sunlight, which proceeds through a free-radical chain in three stages — initiation, propagation and termination.

Initiation Cl₂ →(hν) 2 Cl• Propagation Cl• + CH₄ → CH₃• + HCl CH₃• + Cl₂ → CH₃Cl + Cl• Termination CH₃• + Cl• → CH₃Cl CH₃• + CH₃• → C₂H₆
Free-radical chlorination of methane
Why a mixture forms. Once chlorination starts, the product \(\ce{CH3Cl}\) can itself be attacked, giving \(\ce{CH2Cl2},\ \ce{CHCl3}\) and \(\ce{CCl4}\). The chain nature of the reaction makes clean mono-substitution hard without a large excess of methane.
Section 25-4

Alkenes: Preparation

Alkenes are usually made by elimination — removing two groups from adjacent carbons to create the double bond. When more than one alkene is possible, Saytzeff's rule predicts the more substituted (more stable) alkene as the major product.

MethodReaction
Dehydrohalogenation\(\ce{R-CH2-CH2-X ->[alc. KOH] R-CH=CH2 + HX}\)
Dehydration of alcohol\(\ce{R-CH2-CH2-OH ->[conc. H2SO4][\Delta] R-CH=CH2 + H2O}\)
Dehalogenation\(\ce{R-CHBr-CH2Br + Zn -> R-CH=CH2 + ZnBr2}\)
Section 25-5

Alkenes: Electrophilic Addition

The electron-rich \(\ce{C=C}\) bond is attacked by electrophiles, which add across it. With an unsymmetrical reagent like \(\ce{HX}\), Markovnikov's rule decides the orientation: the hydrogen adds to the carbon that already has more hydrogens, because that route passes through the more stable carbocation.

CH₃–CH=CH₂ + HBr CH₃–CH⁺–CH₃ (2° cation, stable) CH₃–CHBr–CH₃ (2-bromopropane)
Markovnikov addition proceeds through the more stable carbocation
🔁
Markovnikov vs the peroxide effect
\(\ce{HBr}\) alone → Markovnikov · \(\ce{HBr}\) + peroxide → anti-Markovnikov

In the presence of peroxides, \(\ce{HBr}\) adds against Markovnikov (the Kharasch effect) because the mechanism switches to free radicals, forming the more stable radical instead of the more stable cation. This reversal works only for \(\ce{HBr}\), not \(\ce{HCl}\) or \(\ce{HI}\).

ReagentProduct
\(\ce{H2}\) / Nialkane
\(\ce{X2}\)vicinal dihalide
\(\ce{HX}\)haloalkane (Markovnikov)
\(\ce{H2O}\) / \(\ce{H+}\)alcohol (Markovnikov)
Section 25-6

Oxidation & Ozonolysis

Two oxidations of alkenes are classic exam tools. Cold dilute alkaline \(\ce{KMnO4}\) — Baeyer's reagent — gives a diol and decolourises, a quick test for unsaturation. Ozonolysis cleaves the double bond to two carbonyl fragments, revealing where the double bond was.

✂️
Ozonolysis — locating the double bond
\(\ce{R-CH=CH-R' ->[O3][Zn/H2O] R-CHO + R'-CHO}\)

The \(\ce{C=C}\) is split, each carbon becoming a carbonyl. Working backwards from the aldehyde/ketone fragments tells you the structure of the original alkene — a favourite structure-determination trick.

Section 25-7

Alkynes

Alkynes carry a triple bond and undergo addition like alkenes — but the terminal alkyne has a unique trick: its \(\ce{#C-H}\) hydrogen is weakly acidic. The \(sp\)-hybridised carbon has the most \(s\)-character, holding the bonding electrons tightly and stabilising the resulting carbanion.

🔋
Acidity from s-character
\(\ce{HC#CH} > \ce{H2C=CH2} > \ce{CH3-CH3}\) (\(sp > sp^2 > sp^3\))

Terminal alkynes react with sodium to form acetylides: \(\ce{HC#CH + Na -> HC#C-Na+ + \tfrac12 H2}\). With ammoniacal \(\ce{AgNO3}\) or \(\ce{Cu2Cl2}\) they give coloured precipitates — a test that distinguishes terminal from internal alkynes.

ReactionReagentProduct
Hydration (Kucherov)\(\ce{H2O}/\ce{H2SO4}/\ce{HgSO4}\)acetaldehyde (from \(\ce{C2H2}\))
Hydrohalogenation\(\ce{HX}\)vinyl halide → gem-dihalide
Preparation\(\ce{CaC2 + 2H2O}\)\(\ce{C2H2}\) (acetylene)
Section 25-8

Benzene & Aromaticity

Benzene (\(\ce{C6H6}\)) is a planar hexagonal ring with all six \(\ce{C-C}\) bonds of equal length, its six \(\pi\) electrons delocalised in a ring above and below the plane. This delocalisation gives an extra resonance stabilisation that makes aromatic compounds prefer substitution over addition.

6 delocalised π electrons (4n+2, n=1)
Benzene — a fully delocalised aromatic ring
Hückel's rule for aromaticity
planar + cyclic + fully conjugated + \((4n+2)\) \(\pi\) electrons

Benzene has \(6\) \(\pi\) electrons (\(n=1\)), satisfying \(4n+2\). The same test flags aromatic ions and heterocycles; rings with \(4n\) \(\pi\) electrons are anti-aromatic and destabilised.

Section 25-9

Electrophilic Aromatic Substitution

Because the ring is electron-rich, benzene reacts with electrophiles — but rather than add (which would destroy aromaticity), it substitutes, replacing a hydrogen and restoring the ring. Every such reaction follows the same three-step mechanism.

1. generateelectrophile E⁺ 2. arenium ion(σ-complex) 3. lose H⁺aromatic again
The universal EAS mechanism — attack, arenium ion, deprotonation
ReactionReagentElectrophileProduct
Nitrationconc. \(\ce{HNO3}/\ce{H2SO4}\)\(\ce{NO2+}\)nitrobenzene
Halogenation\(\ce{Cl2}/\ce{FeCl3}\)\(\ce{Cl+}\)chlorobenzene
Sulphonationoleum\(\ce{SO3}\)benzenesulphonic acid
F–C alkylation\(\ce{RX}/\ce{AlCl3}\)\(\ce{R+}\)alkylbenzene
F–C acylation\(\ce{RCOCl}/\ce{AlCl3}\)\(\ce{RCO+}\)aryl ketone
Section 25-10

Directing Effects

When benzene already carries a substituent, that group steers the incoming electrophile to particular positions and changes the ring's reactivity. Electron-donating groups activate the ring and direct ortho/para; electron-withdrawing groups deactivate and direct meta.

GroupEffect on ringDirects to
\(\ce{-OH},\ \ce{-NH2},\ \ce{-OR},\ \ce{-CH3}\)activatingortho / para
\(\ce{-NO2},\ \ce{-CN},\ \ce{-COOH},\ \ce{-CHO}\)deactivatingmeta
\(\ce{-Cl},\ \ce{-Br}\) (halogens)deactivatingortho / para
The halogen anomaly. Halogens are the odd ones out: their \(-I\) effect deactivates the ring (so reactions are slower), yet their lone-pair \(+R\) effect directs the electrophile ortho/para. They are the only common deactivating ortho/para directors.
Worked Examples

Putting It to Work

1 Wurtz product

Problem. What alkane forms when bromoethane undergoes the Wurtz reaction?

Solution. Two ethyl units couple:

Working
\[ \ce{2C2H5Br + 2Na -> C4H10 + 2NaBr}\ (\text{butane}) \]
2 A propagation step

Problem. Write a propagation step in the chlorination of methane.

Solution. A chlorine radical abstracts a hydrogen:

Working
\[ \ce{Cl. + CH4 -> CH3. + HCl} \]
3 Markovnikov addition

Problem. Give the major product of \(\ce{CH3-CH=CH2 + HBr}\) (no peroxide).

Solution. H adds to the terminal C; Br to the more substituted C (stable 2° cation):

Working
\[ \ce{CH3-CHBr-CH3}\ (\text{2-bromopropane}) \]
4 Peroxide effect

Problem. What changes if the same reaction is run with \(\ce{HBr}\) and a peroxide?

Solution. Radical mechanism reverses the orientation (anti-Markovnikov):

Working
\[ \ce{CH3-CH2-CH2Br}\ (\text{1-bromopropane}) \]
5 Acidity of alkynes

Problem. Arrange \(\ce{CH3CH3},\ \ce{CH2=CH2},\ \ce{HC#CH}\) by increasing acidity and explain.

Solution. More \(s\)-character holds the lone pair more tightly:

Working
\[ \ce{CH3CH3} < \ce{CH2=CH2} < \ce{HC#CH}\ (sp^3
6 Predict the position

Problem. Where does nitration of nitrobenzene occur, and is the ring more or less reactive than benzene?

Solution. \(\ce{-NO2}\) is a deactivating meta-director:

Working
\[ \text{meta product};\quad \text{ring is } \textit{less} \text{ reactive than benzene} \]
Review

Chapter Summary

Classes

Alkanes (substitution), alkenes & alkynes (addition), aromatics (substitution).

Alkanes

Wurtz, decarboxylation, hydrogenation; free-radical halogenation chain.

Alkenes

Elimination preparations; electrophilic addition; Markovnikov & peroxide effect.

Alkynes

Terminal-H acidity (\(sp\)); acetylides; hydration to carbonyls.

Aromaticity

Planar, cyclic, conjugated, \((4n+2)\) π electrons; benzene has 6.

EAS

Generate E⁺ → arenium ion → lose H⁺; o/p activators vs m deactivators.

Practice

Problems

For each item, first decide which class and reaction type it tests, then apply the relevant mechanism or rule. Difficulty rises down the list.

  1. Classify hydrocarbons and give the general formula of each class.
  2. Write the Wurtz reaction and explain why it suits only symmetrical alkanes.
  3. Give the three stages of the free-radical chlorination of methane with one equation each.
  4. State Saytzeff's rule and apply it to the dehydrohalogenation of 2-bromobutane.
  5. State Markovnikov's rule and predict the product of \(\ce{HBr}\) addition to propene.
  6. Explain the peroxide effect and why it operates only with \(\ce{HBr}\).
  7. What does ozonolysis reveal? Give the products from but-2-ene.
  8. Explain why terminal alkynes are acidic and arrange the acidity of ethane, ethene and ethyne.
  9. How would you distinguish a terminal alkyne from an internal one chemically?
  10. State Hückel's rule and verify that benzene is aromatic.
  11. Outline the three steps of electrophilic aromatic substitution.
  12. Predict the position and relative rate of nitration for (a) phenol and (b) nitrobenzene.
Tip: let bonding dictate the reaction. Single bonds have no exposed electrons, so alkanes only react with radicals (substitution). Double and triple bonds are electron-rich, so they attract electrophiles (addition). Benzene is electron-rich and stabilised, so it attracts electrophiles but keeps its ring (substitution). Identify the bond and the reaction type follows.